methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

Base Information

Chemical Name:methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate
CAS No.:299957-47-4
Molecular Formula:C₂₀H₂₂O₈
Molecular Weight:390.39
Hs Code.:

Synonyms:methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

Suppliers and Price of methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

There total 2 articles about methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 299957-46-3
methyl 2-(2-hydroxy-4-methoxyphenyl)-2-oxoethanoate

: 126809-68-5
2-(methoxymethoxy)-4-methoxybenzyl alcohol

: 299957-47-4
methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/jo0004198

Reference yield:

: 151-10-0
1,3-Dimethoxybenzene

: 299957-47-4
methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / AlCl₃ / 1,2-dichloro-ethane / 24 h / 20 °C

2: 32 percent / DEAD; PPh₃ / dimethylformamide / 24 h / 20 °C

With aluminium trichloride; triphenylphosphine; diethylazodicarboxylate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; 1: Acylation / 2: Mitsunobu reaction;
DOI:10.1021/jo0004198

Reference yield:

: 299957-47-4
methyl 2-(2-methoxymethoxy-4-methoxybenzyloxy)-4-methoxy-phenylglyoxylate

: 479-13-0
coumestrol

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 48 h / 20 °C / Irradiation

2: aq. HCl / tetrahydrofuran / 36 h / 50 °C

3: 75 percent / BBr₃ / CH₂Cl₂ / -78 - 20 °C

With hydrogenchloride; boron tribromide; In tetrahydrofuran; dichloromethane; benzene; 1: Cyclization / 2: Hydrolysis / 3: demethylation;
DOI:10.1021/jo0004198