3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

Base Information

Chemical Name:3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one
CAS No.:917873-61-1
Molecular Formula:C₂₇H₃₀O₃S
Molecular Weight:434.599
Hs Code.:

Synonyms:3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

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Chemical Property of 3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

Chemical Property:

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Technology Process of 3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

There total 7 articles about 3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917873-59-7
3-(4-hydroxy-3,5-dimethyl-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 917873-61-1
3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

Guidance literature:: With sodium hydroxide; In water; isopropyl alcohol; at 20 ℃; for 18h;

Reference yield:

: 4-phenyl-5-propyl-thiophene-2-carboxylic acid methoxy-methyl-amide

: 917873-61-1
3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 3 h

2: hydrogenchloride / ethanol; isopropyl alcohol / 18 h / 20 °C

3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 16 h / 1350.14 Torr

4: sodium hydroxide / water; isopropyl alcohol / 18 h / 20 °C

With hydrogenchloride; sodium hydroxide; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; water; isopropyl alcohol;

Reference yield:

: 21676-88-0
4-phenyl-2-thiophenecarboxylic acid

: 917873-61-1
3-(3,5-dimethyl-4-oxiranylmethoxy-phenyl)-1-(4-phenyl-5-propyl-thiophen-2-yl)-propan-1-one

Guidance literature:: Multi-step reaction with 6 steps

1: tert.-butyl lithium / tetrahydrofuran; pentane / -75 - 20 °C

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C

3: tetrahydrofuran / 3 h

4: hydrogenchloride / ethanol; isopropyl alcohol / 18 h / 20 °C

5: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 16 h / 1350.14 Torr

6: sodium hydroxide / water; isopropyl alcohol / 18 h / 20 °C

With hydrogenchloride; sodium hydroxide; hydrogen; tert.-butyl lithium; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; isopropyl alcohol; pentane;