(4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride

Base Information

• Chemical Name: (4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride
• CAS No.: 952714-70-4
• Molecular Formula: C₁₅H₁₇F₃N₂O₃*ClH
• Molecular Weight: 366.768

Synonyms:(4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride

Chemical Property of (4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride

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Technology Process of (4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride

There total 1 articles about (4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

(S)-3-((2S,3S)-2-azido-4,4,4-trifluoro-3-methylbutanoyl)-4-benzyloxazolidin-2-one (952714-69-1) → (4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride (952714-70-4)

Guidance literature:

With methanolic HCl; hydrogen; palladium 10% on activated carbon; In methanol; under 760.051 Torr;

Reference yield: 86.0%

(4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride (952714-70-4) + 3,4-dichlorobenzenesulphonyl chloride (98-31-7) → (4S)-4-benzyl-3-{(2S,3S)-2-[N-(3,4-dichlorophenylsulfonyl)amino]-3-(trifluoromethyl)butanoyl}-1,3-oxazolidin-2-one (952714-71-5)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

(4S)-4-benzyl-3-[(2S,3S)-2-amino-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one hydrochloride (952714-70-4) → (4S)-4-benzyl-3-[(2S,3S)-2-{N-[4-(trifluoromethyl)benzenesulfonyl]amino}-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one (952714-73-7)

Guidance literature:

In DCM;

upstream raw materials:

(S)-3-((2S,3S)-2-azido-4,4,4-trifluoro-3-methylbutanoyl)-4-benzyloxazolidin-2-one

Downstream raw materials:

(4S)-4-benzyl-3-{(2S,3S)-2-[N-(3,4-dichlorophenylsulfonyl)amino]-3-(trifluoromethyl)butanoyl}-1,3-oxazolidin-2-one

(4S)-4-benzyl-3-[(2S,3S)-2-{N-[4-(trifluoromethyl)benzenesulfonyl]amino}-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one

(4S)-4-benzyl-3-[(2S,3S)-2-{N-(4-fluorophenylsulfonyl)amino}-3-(trifluoromethyl)butanoyl]-1,3-oxazolidin-2-one

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