methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Base Information

Chemical Name:methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside
CAS No.:494800-97-4
Molecular Formula:C₄₀H₅₃NO₁₂
Molecular Weight:739.86
Hs Code.:

Synonyms:methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Suppliers and Price of methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

There total 4 articles about methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 96-32-2
bromoacetic acid methyl ester

: 494800-93-0
methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-(2-aminoethoxy)]ethoxy}ethyl-α,β-D-glucofuranoside

: 494800-97-4
methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Guidance literature:: With triethylamine; In tetrahydrofuran; Heating;
DOI:10.1021/jo025978o

Reference yield:

: 112-26-5,27252-69-3
1,2-bis(2-chloroethoxy)ethane

: 494800-97-4
methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0 - 20 °C

1.2: 87 percent / NaN₃ / dimethylformamide / 4 h / 100 °C

2.1: 50 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3.1: 62 percent / triethylamine / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo025978o

Reference yield:

: 55902-93-7
methyl 3,5,6-tri-O-benzyl-α,β-D-glucofuranoside

: 494800-97-4
methyl 3,5,6-tri-O-benzyl-2-O-{2-[2-[2-N,N-bis(methoxycarbonylmethyl)amino]ethoxy]ethoxy}ethyl-α,β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0 - 20 °C

1.2: 87 percent / NaN₃ / dimethylformamide / 4 h / 100 °C

2.1: 50 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3.1: 62 percent / triethylamine / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo025978o