Technology Process of C39H37F17O6
There total 6 articles about C39H37F17O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: 100 percent / H2 / Pd/C / ethyl acetate / 20 °C
2.1: 100 percent / red-Al; pyrrolidine; t-BuOK / tetrahydrofuran / -20 - 0 °C
3.1: HC(OMe)3; p-TsOH*H2O; Na2SO4 / acetonitrile / 20 °C
3.2: 85 percent / acetonitrile
4.1: 100 percent / KOH / toluene / Heating
5.1: 96 percent / Et3SiH; PhBCl2 / CH2Cl2 / -78 °C
With
pyrrolidine; triethylsilane; potassium hydroxide; phenylborondichloride; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid; sodium sulfate; sodium bis(2-methoxyethoxy)aluminium dihydride; trimethyl orthoformate;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2007.04.106
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94190-74-6
(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-decyl)-triphenyl-phosphonium; iodide
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: 95 percent / K2CO3 / dioxane; H2O / Heating
2.1: 100 percent / H2 / Pd/C / ethyl acetate / 20 °C
3.1: 100 percent / red-Al; pyrrolidine; t-BuOK / tetrahydrofuran / -20 - 0 °C
4.1: HC(OMe)3; p-TsOH*H2O; Na2SO4 / acetonitrile / 20 °C
4.2: 85 percent / acetonitrile
5.1: 100 percent / KOH / toluene / Heating
6.1: 96 percent / Et3SiH; PhBCl2 / CH2Cl2 / -78 °C
With
pyrrolidine; triethylsilane; potassium hydroxide; phenylborondichloride; potassium tert-butylate; hydrogen; potassium carbonate; toluene-4-sulfonic acid; sodium sulfate; sodium bis(2-methoxyethoxy)aluminium dihydride; trimethyl orthoformate;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate; toluene; acetonitrile;
1.1: Wittig reaction;
DOI:10.1016/j.tetlet.2007.04.106