Technology Process of 3-chloro-5-methoxyphenyl 4-chlorophenyl sulfide
There total 2 articles about 3-chloro-5-methoxyphenyl 4-chlorophenyl sulfide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-chloro-3-methoxy-benzene;
With
(1,5-cyclooctadiene)(methoxy)iridium(I) dimer; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
tetrahydrofuran;
at 80 ℃;
for 24h;
Inert atmosphere;
4,4'-dichlorodiphenyl disulfide;
With
[2,2]bipyridinyl; copper(l) chloride;
In
water; dimethyl sulfoxide;
at 80 ℃;
for 24h;
regioselective reaction;
Inert atmosphere;
DOI:10.1039/c2cc33950a
- Guidance literature:
-
1-chloro-3-methoxy-benzene;
With
(1,5-cyclooctadiene)(methoxy)iridium(I) dimer; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
tetrahydrofuran;
at 80 ℃;
for 24h;
Schlenk technique;
Inert atmosphere;
p-Chlorothiophenol;
With
pyridine; copper diacetate;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 24h;
regioselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/ejoc.201300248
