trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4

Base Information

Chemical Name:trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4
CAS No.:113088-85-0
Molecular Formula:C₂₄H₂₀B*C₅₂H₅₁FeP₄
Molecular Weight:1174.95
Hs Code.:

Synonyms:trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4

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Chemical Property of trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4

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Technology Process of trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4

There total 2 articles about trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 19392-93-9,32490-70-3
trans-hydridochloro-di-{1,2-bis(diphenylphosphino)ethane}iron(II)

: 143-66-8
sodium tetraphenyl borate

: 113088-85-0
trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4

Guidance literature:: With H₂; In tetrahydrofuran; ethanol; byproducts: NaCl; dissoln. of Fe-complex in THF/EtOH, addn. of a soln. of NaBPh4/EtOH under H2 to this deep purple soln., after 10 min color change to pink, stirring for 12 h (color change to cloudy yellow); filtration, washing with benzene, then H2O, then diethyl ether;

Reference yield:

: 109750-49-4
{Fe(.eta2-H₂)(H)(PPh₂CH₂CH₂PPh₂)2}BF₄

: 143-66-8
sodium tetraphenyl borate

: 113088-85-0
trans-(Fe(η2-H2)(H)(Ph2PCH2CH2PPh2)2)BPh4

Guidance literature:: In methanol; dichloromethane; solution of Fe-compound was filtered into the tube, methanol was carefully added, 20°C, reactiontime: 1-3 days;
DOI:10.1021/ja00206a009