2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

Base Information

Chemical Name:2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid
CAS No.:796072-02-1
Molecular Formula:C₃₄H₃₃NO₅
Molecular Weight:535.64
Hs Code.:

Synonyms:2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

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Chemical Property of 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

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Technology Process of 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

There total 10 articles about 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 796072-32-7
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid methyl ester

: 796072-02-1
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

Guidance literature:: 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid methyl ester; With methanol; potassium hydroxide; water; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=2;

Reference yield:

: 796072-31-6
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentenoic acid methyl ester

: 796072-02-1
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1 h / 1034.32 Torr / Parr apperatous

2: potassium hydroxide; water / tetrahydrofuran; methanol / 1 h / 0 - 20 °C

With potassium hydroxide; water; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethyl acetate;

Reference yield:

: 796072-24-7
(4-dibenzofuran-4-yl-phenyl)-trimethyl-silane

: 796072-02-1
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C

1.2: 2.5 h / -78 - 20 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 2 h / Heating / reflux

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1 h / 1034.32 Torr / Parr apperatous

4.1: potassium hydroxide; water / tetrahydrofuran; methanol / 1 h / 0 - 20 °C

With potassium hydroxide; water; hydrogen; boron tribromide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; 2.1: Suzuki Coupling;