3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

Base Information

Chemical Name:3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole
CAS No.:1314970-14-3
Molecular Formula:C₂₆H₃₁I₂NO₃
Molecular Weight:659.346
Hs Code.:

Synonyms:3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

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Chemical Property of 3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

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Technology Process of 3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

There total 5 articles about 3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1314969-99-7
3,3-di(but-3-enyl)-2,3-dihydro-1H-indole

: 1314970-12-1
1-chloromethyl-2,6-diiodo-3,4,5-trimethoxybenzene

: 1314970-14-3
3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; for 16h; Inert atmosphere; Reflux;
DOI:10.1039/c1ob05527e

Reference yield:

: 1314969-95-3
tert-butyl 3,3-di(but-3-enyl)-2-oxo-2,3-dihydroindole-1-carboxylate

: 1314970-14-3
3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 70 °C / Inert atmosphere

3: potassium carbonate; potassium iodide / acetone / 16 h / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; potassium carbonate; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1039/c1ob05527e

Reference yield:

: 1314970-11-0
(2,6-diiodo-3,4,5-trimethoxyphenyl)methanol

: 1314970-14-3
3,3-di(but-3-enyl)-1-(2,6-diiodo-3,4,5-trimethoxybenzyl)-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetone / 16 h / Inert atmosphere; Reflux

With thionyl chloride; potassium carbonate; potassium iodide; In dichloromethane; acetone;
DOI:10.1039/c1ob05527e