3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

Base Information

Chemical Name:3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone
CAS No.:308845-82-1
Molecular Formula:C₂₇H₂₄ClN₃O₃
Molecular Weight:473.959
Hs Code.:

Synonyms:3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

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Chemical Property of 3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

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Technology Process of 3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

There total 5 articles about 3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 64-04-0
phenethylamine

: 308845-81-0
2-(3,5-dichloro-2-oxo-6-phenylpyrazin-1(2H)-yl)acetic acid benzyl ester

: 308845-82-1
3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

Guidance literature:: In ethyl acetate; at 20 ℃; for 18h; Heating / reflux;

Reference yield:

: 1738-68-7
Gly-OBz

: 308845-82-1
3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

Guidance literature:: Multi-step reaction with 2 steps

1.1: CH₂Cl₂

1.2: 1,2-dichloro-benzene

2.1: acetonitrile / 70 °C

In dichloromethane; acetonitrile;
DOI:10.1021/jm030131l

Reference yield:

: 757971-35-0
benzyl N (1-cyanobenzyl)glycine hydrochloride

: 308845-82-1
3-(2-phenylethylamino)-5-chloro-6-phenyl-1-benzyloxycarbonylmethylpyrazinone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,2-dichloro-benzene / 18 h / 20 - 100 °C

2: ethyl acetate / 18 h / 20 °C / Heating / reflux

With hydrogenchloride; In ethyl acetate; 1,2-dichloro-benzene;