C₃₂H₅₂O₆Si₂

Base Information

Chemical Name:C₃₂H₅₂O₆Si₂
CAS No.:1401427-10-8
Molecular Formula:C₃₂H₅₂O₆Si₂
Molecular Weight:588.932
Hs Code.:

C<sub>32</sub>H<sub>52</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₂H₅₂O₆Si₂

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Chemical Property of C₃₂H₅₂O₆Si₂

Chemical Property:

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Technology Process of C₃₂H₅₂O₆Si₂

There total 11 articles about C₃₂H₅₂O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1401427-09-5
C₂₉H₄₄O₆Si

: 1401427-10-8
C₃₂H₅₂O₆Si₂

Guidance literature:: C₂₉H₄₄O₆Si; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.0333333h; Inert atmosphere;

trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja307207q

Reference yield:

: 1401427-03-9
C₂₈H₄₀O₅Si

: 1401427-10-8
C₃₂H₅₂O₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethylzinc / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 - 0 °C / Inert atmosphere

1.3: 0.33 h / -78 - -20 °C / Inert atmosphere

2.1: cerium(III) chloride; lithium chloride / diethyl ether; tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2.2: 2.5 h / -78 - 0 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / benzene / 3.17 h / 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / -78 - -5 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 4 h / -78 °C / Inert atmosphere

6.2: 0.67 h / -78 - 0 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.03 h / 0 °C / Inert atmosphere

7.2: 1 h / 0 - 20 °C / Inert atmosphere

With cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; diethylzinc; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; benzene;
DOI:10.1021/ja307207q

Reference yield:

: C₃₁H₅₀O₅Si₂

: 1401427-10-8
C₃₂H₅₂O₆Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: diethylzinc / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 0 °C / Inert atmosphere

2.3: 0.33 h / -78 - -20 °C / Inert atmosphere

3.1: cerium(III) chloride; lithium chloride / diethyl ether; tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

3.2: 2.5 h / -78 - 0 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / benzene / 3.17 h / 20 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / -78 - -5 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 4 h / -78 °C / Inert atmosphere

7.2: 0.67 h / -78 - 0 °C / Inert atmosphere

8.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.03 h / 0 °C / Inert atmosphere

8.2: 1 h / 0 - 20 °C / Inert atmosphere

With cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; diethylzinc; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; benzene;
DOI:10.1021/ja307207q