1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

Base Information

Chemical Name:1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester
CAS No.:741606-13-3
Molecular Formula:C₃₂H₄₃NO₅
Molecular Weight:521.697
Hs Code.:

Synonyms:1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

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Chemical Property of 1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

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Technology Process of 1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

There total 5 articles about 1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 741606-02-0
[1-bromo-3-(4-octylphenoxy)propan-2-yl]acetate

: 741606-13-3
1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

Guidance literature:: tert-butyl 1H-indole-3-carboxylate; With potassium tert-butylate; In dimethyl sulfoxide; at 110 ℃; for 0.25h;

[1-bromo-3-(4-octylphenoxy)propan-2-yl]acetate; In dimethyl sulfoxide; at 110 ℃; for 0.5h;

Reference yield:

: 741606-02-0
[1-bromo-3-(4-octylphenoxy)propan-2-yl]acetate

: 61698-94-0
tert-butyl 1H-indole-3-carboxylate

: 741606-13-3
1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

Guidance literature:: 1H-indole-3-carboxylic tert-butyl ester; With potassium tert-butylate; In dimethyl sulfoxide; at 110 ℃; for 0.25h;

[1-bromo-3-(4-octylphenoxy)propan-2-yl]acetate; In dimethyl sulfoxide; at 110 ℃; for 0.5h;
DOI:10.1021/jm051243a

Reference yield:

: 741606-01-9
1-bromo-3-(4-octylphenoxy)propan-2-ol

: 741606-13-3
1-[2-acetoxy-3-(4-octylphenoxy)propyl]indole-3-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 99 percent / pyridine / CH₂Cl₂ / 3.5 h / 0 °C

2.1: potassium tert-butylate / dimethylsulfoxide / 0.25 h / 110 °C

2.2: dimethylsulfoxide / 0.5 h / 110 °C

With pyridine; potassium tert-butylate; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm051243a