bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

Base Information

Chemical Name:bis(3-hydroxy-4-isopropyloxyphenylethyl)amine
CAS No.:99896-52-3
Molecular Formula:C₂₂H₃₁NO₄
Molecular Weight:373.492
Hs Code.:

Synonyms:bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

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Technology Process of bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

There total 9 articles about bis(3-hydroxy-4-isopropyloxyphenylethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99896-49-8
bis(3-benzyloxy-4-isopropyloxyphenylethyl)amine

: 99896-52-3
bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; under 735.5 Torr; Ambient temperature;

Reference yield:

: 94283-73-5
3-hydroxy-4-isopropoxy benzaldehyde

: 99896-52-3
bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / K₂CO₃ / dimethylformamide / 1.5 h / Heating

2: 86 percent / ammonium acetate / acetic acid / 3 h / Heating

3: 90 percent / LiAlH₄ / tetrahydrofuran; diethyl ether

4: 78 percent / 2 h / 180 °C

5: 67 percent / HCl, NaBH₄ / tetrahydrofuran / 6 h / Heating

6: conc. HCl, H₂ / 10percent Pd/C / ethanol / 735.5 Torr / Ambient temperature

With ammonium acetate; hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 99896-31-8
3-benzyloxy-4-isopropyloxybenzaldehyde

: 99896-52-3
bis(3-hydroxy-4-isopropyloxyphenylethyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / ammonium acetate / acetic acid / 3 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran; diethyl ether

3: 78 percent / 2 h / 180 °C

4: 67 percent / HCl, NaBH₄ / tetrahydrofuran / 6 h / Heating

5: conc. HCl, H₂ / 10percent Pd/C / ethanol / 735.5 Torr / Ambient temperature

With ammonium acetate; hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; acetic acid;