(4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

Base Information

Chemical Name:(4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate
CAS No.:1402544-91-5
Molecular Formula:C₁₆H₂₈N₂O₃
Molecular Weight:296.41
Hs Code.:

Synonyms:(4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

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Chemical Property of (4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

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Technology Process of (4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

There total 5 articles about (4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1402544-90-4
(4R,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-nitrocyclohex-1-enecarboxylate

: 1402544-91-5
(4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

Guidance literature:: With chloro-trimethyl-silane; zinc; In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201200093

Reference yield:

: 113981-99-0
C₁₃H₂₃NO₃

: 1402544-91-5
(4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

4: chloro-trimethyl-silane; zinc / ethanol / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; zinc; In ethanol; dichloromethane;
DOI:10.1002/adsc.201200093

Reference yield:

: 1402544-89-1
(4R,5S)-ethyl 4-{(S)-1-[(tert-butoxycarbonyl)amino]-3-methylbutyl}-5-nitrocyclohex-1-enecarboxylate

: 1402544-91-5
(4S,5S)-ethyl 4-[(S)-1-acetamido-3-methylbutyl]-5-aminocyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

3: chloro-trimethyl-silane; zinc / ethanol / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; zinc; In ethanol; dichloromethane;
DOI:10.1002/adsc.201200093