C₆₃H₇₈N₄O₁₁

Base Information

• Chemical Name: C₆₃H₇₈N₄O₁₁
• CAS No.: 1351476-37-3
• Molecular Formula: C₆₃H₇₈N₄O₁₁
• Molecular Weight: 1067.33
• Mol file: 1351476-37-3.mol

Synonyms:C₆₃H₇₈N₄O₁₁

Chemical Property of C₆₃H₇₈N₄O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₃H₇₈N₄O₁₁

There total 6 articles about C₆₃H₇₈N₄O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

C24H21N3O9 (1351476-36-2) + C39H59NO3 (1351476-31-7) → C63H78N4O11 (1351476-37-3)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; chloroform; at 20 ℃; for 3h;

DOI:10.1002/anie.201104099

Reference yield:

C17H27BrO (1351476-28-2) → C63H78N4O11 (1351476-37-3)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium hydroxide / ethanol / 4 h / Reflux

2: potassium carbonate / acetonitrile / 20 h / Reflux

3: hydrazine hydrate / ethanol / 3 h / Reflux

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; chloroform / 3 h / 20 °C

With dmap; potassium carbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In tetrahydrofuran; ethanol; chloroform; acetonitrile;

DOI:10.1002/anie.201104099

Reference yield:

C47H61NO5 (1351476-30-6) → C63H78N4O11 (1351476-37-3)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; chloroform / 3 h / 20 °C

With dmap; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; chloroform;

DOI:10.1002/anie.201104099

upstream raw materials:

1,5-dibromo-pentane

C₁₇H₂₇BrO

C₂₇H₃₄O₃

C₄₇H₆₁NO₅

Downstream raw materials:

C₆₃H₈₀N₄O₉