C₂₈H₄₈O₅Si

Base Information

Chemical Name:C₂₈H₄₈O₅Si
CAS No.:1300040-17-8
Molecular Formula:C₂₈H₄₈O₅Si
Molecular Weight:492.772
Hs Code.:

C<sub>28</sub>H<sub>48</sub>O<sub>5</sub>Si

Synonyms:C₂₈H₄₈O₅Si

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Chemical Property of C₂₈H₄₈O₅Si

Chemical Property:

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Technology Process of C₂₈H₄₈O₅Si

There total 3 articles about C₂₈H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₄O₅

: 69739-34-0
t-butyldimethylsiyl triflate

: 1300040-17-8
C₂₈H₄₈O₅Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at -10 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.02.061

Reference yield:

: 1300040-10-1
C₂₃H₃₂O₅

: 1300040-17-8
C₂₈H₄₈O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 40 °C

1.2: 20 °C

2.1: triethyl borane; oxygen; tri-n-butyl-tin hydride / toluene / -30 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; triethyl borane; oxygen; tri-n-butyl-tin hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1016/j.tet.2011.02.061

Reference yield:

: C₂₂H₂₉IO₅

: 1300040-17-8
C₂₈H₄₈O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: triethyl borane; oxygen; tri-n-butyl-tin hydride / toluene / -30 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; triethyl borane; oxygen; tri-n-butyl-tin hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.02.061