2-[6-(acetyloxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromen-2-yl]-N,N,N-trimethylethanaminium 4-methylbenzenesulfonate

Base Information

Chemical Name:2-[6-(acetyloxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromen-2-yl]-N,N,N-trimethylethanaminium 4-methylbenzenesulfonate
CAS No.:128008-97-9
Molecular Formula:C27H39NO6S
Molecular Weight:505.6667
Hs Code.:
Mol file:128008-97-9.mol

Synonyms:

Suppliers and Price of 2-[6-(acetyloxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromen-2-yl]-N,N,N-trimethylethanaminium 4-methylbenzenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of 2-[6-(acetyloxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromen-2-yl]-N,N,N-trimethylethanaminium 4-methylbenzenesulfonate

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[6-(acetyloxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromen-2-yl]-N,N,N-trimethylethanaminium 4-methylbenzenesulfonate

There total 3 articles about 2-[6-(acetyloxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromen-2-yl]-N,N,N-trimethylethanaminium 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 130266-64-7
3,4-Dihydro-2-(2-dimethylaminoethyl)-2,5,7,8-tetramethyl-2H-benzopyran-6-yl acetate

: 80-48-8
methyl p-toluene sulfonate

: 128008-97-9
6-acetyloxy-3,4-dihydro-N,N,N,2,5,7,8-heptamethyl-2H-1-benzopyran-2-ethanaminium 4-methylbenzenesulfonate

Guidance literature:: In acetonitrile; for 4h; Heating;
DOI:10.1021/jm00105a040

Reference yield:

: 130266-63-6
3,4-Dihydro-2-(2-bromoethyl)-2,5,7,8-tetramethyl-2H-1-benzopyran-6-yl acetate

: 128008-97-9
6-acetyloxy-3,4-dihydro-N,N,N,2,5,7,8-heptamethyl-2H-1-benzopyran-2-ethanaminium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / dimethylformamide / Ambient temperature; overnight

2: 86 percent / acetonitrile / 4 h / Heating

In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00105a040