Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

Base Information

Chemical Name:Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine
CAS No.:1319016-78-8
Molecular Formula:C₆₄H₄₆N₂
Molecular Weight:843.083
Hs Code.:

Synonyms:Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

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Chemical Property of Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

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Technology Process of Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

There total 8 articles about Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 589-87-7
1,4-bromoiodobenzene

: 1398654-34-6
N-allyl-N-(3-(4-bromophenyl)prop-2-yn-1-yl)methanesulfonamide

: 1319016-78-8
Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

: 1353025-93-0
C₄₄H₃₂N₂

: 1219958-87-8
C₃₂H₂₁NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 7 h / 0 °C / Schlenk technique; Inert atmosphere

1.2: Schlenk technique; Reflux; Inert atmosphere

2.1: sodium hydroxide / toluene / 0.5 h / Inert atmosphere; Reflux

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; sodium hydroxide; In toluene;
DOI:10.1039/c2dt31825c

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 589-87-7
1,4-bromoiodobenzene

: 1398654-34-6
N-allyl-N-(3-(4-bromophenyl)prop-2-yn-1-yl)methanesulfonamide

: 1319016-78-8
Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

: 1353025-93-0
C₄₄H₃₂N₂

: 1219958-87-8
C₃₂H₂₁NO

: 1338250-05-7
dimethyl 4-iodophenylboronate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 7 h / 0 °C / Schlenk technique; Inert atmosphere

1.2: Schlenk technique; Reflux; Inert atmosphere

2.1: sodium hydroxide / toluene / 0.5 h / Inert atmosphere; Reflux

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; sodium hydroxide; In toluene;
DOI:10.1039/c2dt31825c

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 589-87-7
1,4-bromoiodobenzene

: 1398654-34-6
N-allyl-N-(3-(4-bromophenyl)prop-2-yn-1-yl)methanesulfonamide

: 1319016-78-8
Biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-[4-(8,8-diphenyl-8H-indolo[3,2,1-de]acridin-3-yl)phenyl]amine

: 1353025-93-0
C₄₄H₃₂N₂

: 1219958-87-8
C₃₂H₂₁NO

: 1338250-05-7
dimethyl 4-iodophenylboronate

: 607739-89-9
C₃₈H₂₆N₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 7 h / 0 °C / Schlenk technique; Inert atmosphere

1.2: Schlenk technique; Reflux; Inert atmosphere

2.1: sodium hydroxide / toluene / 0.5 h / Inert atmosphere; Reflux

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; sodium hydroxide; In toluene;
DOI:10.1039/c2dt31825c