N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester

Base Information

• Chemical Name: N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester
• CAS No.: 353757-39-8
• Molecular Formula: C₃₁H₃₅ClN₂O₅
• Molecular Weight: 551.082

Synonyms:N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester

Chemical Property of N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester

There total 2 articles about N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methoxyfenoside (161050-58-4,163442-56-6) + C9H8Cl2O2 (400848-56-8) → N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester (353757-39-8)

Guidance literature:

methoxyfenoside; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃;

C₉H₈Cl₂O₂; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1016/S0040-4039(01)01644-6

Reference yield:

2-methylphenyl aldehyde (529-20-4) → N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester (353757-39-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine / diethyl ether / 2 h / 20 °C

2.1: potassium tert-butoxide / tetrahydrofuran / 20 °C

2.2: tetrahydrofuran / 4 h / 20 °C

With pyridine; potassium tert-butylate; In tetrahydrofuran; diethyl ether;

DOI:10.1016/S0040-4039(01)01644-6

Reference yield: 65.0%

acetic acid (64-19-7,77671-22-8) + N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester (353757-39-8) → acetic acid [N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinocarbonyloxy]-o-tolyl-methyl ester

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

DOI:10.1016/S0040-4039(01)01644-6

upstream raw materials:

methoxyfenoside

C₉H₈Cl₂O₂

2-methylphenyl aldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 353757-39-8 N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send