5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Base Information

Chemical Name:5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide
CAS No.:1618132-15-2
Molecular Formula:C₄₀H₄₇N₄O*I
Molecular Weight:726.744
Hs Code.:

5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Synonyms:5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

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Chemical Property of 5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

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Technology Process of 5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

There total 2 articles about 5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1618132-14-1
5-acetylamino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-acetylaminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

: 1618132-15-2
5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Guidance literature:: With boron trifluoride methanol complex; In methanol; Reflux;
DOI:10.1016/j.dyepig.2014.05.002

Reference yield:

: 63857-00-1,70446-42-3
N-[(3-(anilinomethylene)-2-chloro-1-cyclohexen-1-yl)methylene]aniline hydrochloride

: 1618132-15-2
5-amino-2-[2-[3-[2-(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-indol-2-ylidene)ethylidene]-2-(4-aminophenoxy)-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-3H-indolium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; acetic acid

2: sodium acetate / methanol / 0.17 h / Reflux

3: methanol; mineral oil / 6 h / 60 °C

4: boron trifluoride methanol complex / methanol / Reflux

With sodium acetate; boron trifluoride methanol complex; acetic acid; triethylamine; In methanol; mineral oil;
DOI:10.1016/j.dyepig.2014.05.002