4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

Base Information

Chemical Name:4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline
CAS No.:202392-85-6
Molecular Formula:C₃₂H₃₄F₁₃N₃O₄S
Molecular Weight:803.685
Hs Code.:

Synonyms:4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

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Chemical Property of 4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

Chemical Property:

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Technology Process of 4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

There total 3 articles about 4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-(8-hydroxyoctyl)aniline

: 920-46-7,26937-45-1
Methacryloyl chloride

: 202392-85-6
4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃;
DOI:10.1246/bcsj.70.3153

Reference yield:

: 147029-28-5
4-(Perfluorohexylsulfonyl)aniline

: 202392-85-6
4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: conc. hydrochloric acid; sodium nitrite / acetone; H₂O / 1 h / 0 °C

1.2: 68 percent / acetone; H₂O / 2 h / 0 °C

2.1: 52 percent / triethylamine / tetrahydrofuran / 0 °C

With hydrogenchloride; triethylamine; sodium nitrite; In tetrahydrofuran; water; acetone; 1.1: Diazotization / 1.2: coupling / 2.1: Acylation;
DOI:10.1246/bcsj.70.3153

Reference yield:

: 8-(ethyl-phenyl-amino)-octan-1-ol

: 202392-85-6
4-[4-(perflurohexylsulfonyl)phenylazo]-N-ethyl-N-[8-(methacryloyloxy)octyl]aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: conc. hydrochloric acid; sodium nitrite / acetone; H₂O / 1 h / 0 °C

1.2: 68 percent / acetone; H₂O / 2 h / 0 °C

2.1: 52 percent / triethylamine / tetrahydrofuran / 0 °C

With hydrogenchloride; triethylamine; sodium nitrite; In tetrahydrofuran; water; acetone; 1.1: Diazotization / 1.2: coupling / 2.1: Acylation;
DOI:10.1246/bcsj.70.3153