Technology Process of C36H21BrN4S4
There total 6 articles about C36H21BrN4S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
chloroform; N,N-dimethyl-formamide;
at 60 ℃;
for 4h;
Inert atmosphere;
DOI:10.1002/anie.201201265
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1.25 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium acetate; bis(pinacol)diborane; XPhos / 1,4-dioxane / 1 h / 110 °C / Inert atmosphere
2.2: 24 h / 40 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
3.2: 1 h / -78 - 20 °C / Inert atmosphere
3.3: 24 h / 80 °C / Inert atmosphere
4.1: N-Bromosuccinimide / chloroform; N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; N-Bromosuccinimide; n-butyllithium; potassium acetate; bis(pinacol)diborane; lithium diisopropyl amide; XPhos;
In
tetrahydrofuran; 1,4-dioxane; hexane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/anie.201201265
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide / chloroform / 18 h / 60 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 - 20 °C / Inert atmosphere
2.3: 24 h / 80 °C / Inert atmosphere
3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 27 h / 60 °C / Inert atmosphere
4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
4.2: 1 h / -78 - 20 °C / Inert atmosphere
4.3: 24 h / 80 °C / Inert atmosphere
5.1: N-Bromosuccinimide / chloroform; N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere
With
N-Bromosuccinimide; n-butyllithium;
In
tetrahydrofuran; hexane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/anie.201201265