C₁₀H₁₄NO₄P

Base Information

Chemical Name:C₁₀H₁₄NO₄P
CAS No.:1369491-73-5
Molecular Formula:C₁₀H₁₄NO₄P
Molecular Weight:243.199
Hs Code.:

C<sub>10</sub>H<sub>14</sub>NO<sub>4</sub>P

Synonyms:C₁₀H₁₄NO₄P

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Chemical Property of C₁₀H₁₄NO₄P

Chemical Property:

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Technology Process of C₁₀H₁₄NO₄P

There total 1 articles about C₁₀H₁₄NO₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 29681-38-7
methyl 5-methylpyridine-2-carboxylate

: 756-79-6
dimethyl methane phosphonate

: 1369491-73-5
C₁₀H₁₄NO₄P

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h; Inert atmosphere;

methyl 5-methylpyridine-2-carboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; hexane; water;
DOI:10.1021/ol300541u

Reference yield:

: 1369491-73-5
C₁₀H₁₄NO₄P

: C₁₆H₁₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / 1,2-dimethoxyethane; toluene / 2 h / -20 °C / Inert atmosphere

2: hydroquinone / toluene / 46 h / 155 °C / Inert atmosphere

With potassium tert-butylate; hydroquinone; In 1,2-dimethoxyethane; toluene; 2: Diels-Alder reaction;
DOI:10.1021/ol300541u

Reference yield:

: 1369491-73-5
C₁₀H₁₄NO₄P

: C₁₄H₁₅NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / 1,2-dimethoxyethane; toluene / 2 h / -20 °C / Inert atmosphere

2: hydroquinone / toluene / 46 h / 155 °C / Inert atmosphere

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 19 h / 75 °C

With lithium hydroxide monohydrate; potassium tert-butylate; water; hydroquinone; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; toluene; 2: Diels-Alder reaction;
DOI:10.1021/ol300541u