CHS-Met-Leu-Phe-OMe

Base Information

Chemical Name:CHS-Met-Leu-Phe-OMe
CAS No.:99701-27-6
Molecular Formula:C₂₂H₃₃N₃O₄S₂
Molecular Weight:467.654
Hs Code.:

Synonyms:CHS-Met-Leu-Phe-OMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CHS-Met-Leu-Phe-OMe

Chemical Property:

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Technology Process of CHS-Met-Leu-Phe-OMe

There total 3 articles about CHS-Met-Leu-Phe-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 77543-00-1,65929-03-5
N-formylmethionylleucylphenylalanine methyl ester

: 99701-27-6
CHS-Met-Leu-Phe-OMe

Guidance literature:: With thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide); In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1139/v85-511

Reference yield:

: 77542-78-0
Boc-Met-Leu-Phe-OMe

: 99701-27-6
CHS-Met-Leu-Phe-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: 98percent formic acid / 3 h / Ambient temperature

2: EEDQ / CHCl₃ / 8 h / Ambient temperature

3: 70 percent / thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide) / tetrahydrofuran / 1 h / 0 °C

With formic acid; thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide); N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; chloroform;
DOI:10.1139/v85-511

Reference yield:

: 77542-94-0
H-Met-Leu-Phe-OMe formate salt

: 99701-27-6
CHS-Met-Leu-Phe-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: EEDQ / CHCl₃ / 8 h / Ambient temperature

2: 70 percent / thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide) / tetrahydrofuran / 1 h / 0 °C

With thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide); N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; chloroform;
DOI:10.1139/v85-511