p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside
CAS No.:1332838-84-2
Molecular Formula:C₂₆H₃₉NO₁₆
Molecular Weight:621.593
Hs Code.:

Synonyms:p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

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Chemical Property of p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

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Technology Process of p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

There total 7 articles about p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1332839-02-7
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-4-O-acetyl-6-O-benzoyl-3-O-(2,3,4-tri-O-acetyl-α-L-arabinopyranosyl)-β-D-galactopyranoside

: 1332838-84-2
p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 5h;
DOI:10.1016/j.tetasy.2011.06.025

Reference yield:

: 1332838-94-4
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->2)-6-O-benzoyl-β-D-galactopyranoside

: 1332838-84-2
p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: camphor-10-sulfonic acid / acetonitrile / 1 h / 20 °C

1.2: 0.75 h / 20 °C

2.1: N-iodo-succinimide; lanthanum(lll) triflate / dichloromethane / 1 h / 15 °C / Molecular sieve; Inert atmosphere

3.1: hydrazine hydrate / ethanol / 12 h / 80 °C

3.2: 12 h / 20 °C

4.1: sodium methylate / methanol / 5 h / 20 °C

With N-iodo-succinimide; camphor-10-sulfonic acid; sodium methylate; hydrazine hydrate; lanthanum(lll) triflate; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tetasy.2011.06.025

Reference yield:

: 1332838-92-2
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->2)-6-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

: 1332838-84-2
p-methoxyphenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-(α-L-arabinopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid / water / 2 h / 80 °C

2.1: camphor-10-sulfonic acid / acetonitrile / 1 h / 20 °C

2.2: 0.75 h / 20 °C

3.1: N-iodo-succinimide; lanthanum(lll) triflate / dichloromethane / 1 h / 15 °C / Molecular sieve; Inert atmosphere

4.1: hydrazine hydrate / ethanol / 12 h / 80 °C

4.2: 12 h / 20 °C

5.1: sodium methylate / methanol / 5 h / 20 °C

With N-iodo-succinimide; camphor-10-sulfonic acid; sodium methylate; hydrazine hydrate; acetic acid; lanthanum(lll) triflate; In methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetasy.2011.06.025