Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester
CAS No.:51363-93-0
Molecular Formula:C₂₂H₂₉F₉O₃S
Molecular Weight:544.522
Hs Code.:

Synonyms:Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

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Chemical Property of Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

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Technology Process of Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

There total 1 articles about Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-59-9
p-toluenesulfonyl chloride

: 36096-97-6
12,12,13,13,14,14,15,15,15-nonafluoro-1-pentadecanol

: 51363-93-0
Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

Guidance literature:: With pyridine; at -15 ℃; for 5h;
DOI:10.1002/hlca.19960790209

Reference yield:

: 13071-59-5,17325-85-8,56552-80-8,4799-67-1
3-benzyloxypropan-1,2-diol

: 51363-93-0
Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

: 134073-91-9
[2,3-Bis-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; for 72h; Heating;
DOI:10.1002/hlca.19960790209

Reference yield:

: 51363-93-0
Toluene-4-sulfonic acid 12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyl ester

: Phosphoric acid 2,3-bis-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propyl ester 2-bromo-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 12N KOH, Bu₄N(HSO₄) / diethyl ether / 72 h / Heating

2: 100 percent / H₂, AcOH / 10percent Pd/C / ethanol / 1140 Torr

3: Et₃N / diethyl ether / 0 deg C then room t., 12 h and 4 h, reflux

4: H₂O / diethyl ether / 17 h / Ambient temperature

With potassium hydroxide; water; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; acetic acid; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1002/hlca.19960790209