cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

Base Information

Chemical Name:cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane
CAS No.:875461-74-8
Molecular Formula:C₄₅H₆₅N₃O₄
Molecular Weight:712.029
Hs Code.:

Synonyms:cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

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Chemical Property of cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

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Technology Process of cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

There total 3 articles about cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 866719-38-2
1-(3,5-dimethoxybenzylamino)-3,5-diaminocyclohexane

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 875461-74-8
cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

Guidance literature:: With 3 A molecular sieve; In methanol; for 24h; Heating;
DOI:10.1016/j.tetlet.2005.07.112

Reference yield:

: 174542-27-9
cis,cis-1,3,5-tris(3,5-dimethoxybenzylideneamino)cyclohexane

: 875461-74-8
cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Ni(NO₃)2*6H₂O / CH₂Cl₂; methanol / 18 h

1.2: NaBH₄ / methanol / 0.5 h / Heating

1.3: NaCN / H₂O / 2 h / Heating

2.1: 92 percent / 3 Angstroem molecular sieves / methanol / 24 h / Heating

With 3 A molecular sieve; nickel(II) nitrate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2005.07.112

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 875461-74-8
cis-1-(3,5-di-methoxybenzylideneamino)-3,5-[2-hydroxy-(3,5-di-tertbutyl)benzylideneimino]cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / NaOH / H₂O; diethyl ether / 24 h

2.1: Ni(NO₃)2*6H₂O / CH₂Cl₂; methanol / 18 h

2.2: NaBH₄ / methanol / 0.5 h / Heating

2.3: NaCN / H₂O / 2 h / Heating

3.1: 92 percent / 3 Angstroem molecular sieves / methanol / 24 h / Heating

With sodium hydroxide; 3 A molecular sieve; nickel(II) nitrate; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1016/j.tetlet.2005.07.112