3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

Base Information

Chemical Name:3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride
CAS No.:120634-21-1
Molecular Formula:C₁₈H₁₈N₂S₂*ClH
Molecular Weight:362.947
Hs Code.:

Synonyms:3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

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Chemical Property of 3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

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Technology Process of 3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

There total 3 articles about 3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 120634-32-4,120634-33-5
(Z)-3-Amino-3-benzylsulfanyl-2-benzylsulfanylmethyl-acrylonitrile

: 120634-21-1
3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 2.25h; Ambient temperature;
DOI:10.1055/s-1988-27719

Reference yield:

: 19607-38-6
2-[bis(benzylsulfanyl)methylidene]malononitrile

: 120634-21-1
3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / NaBH₄ / ethanol / 0.5 h / 0 °C

2: 100 percent / HCl / diethyl ether / 2.25 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; In diethyl ether; ethanol;
DOI:10.1055/s-1988-27719

Reference yield:

: 100-44-7
benzyl chloride

: 120634-21-1
3-Benzylsulfanyl-2-cyano-thiopropionimidic acid benzyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

2: 48 percent / NaBH₄ / ethanol / 0.5 h / 0 °C

3: 100 percent / HCl / diethyl ether / 2.25 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; In diethyl ether; ethanol;
DOI:10.1055/s-1988-27719