2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

Base Information

Chemical Name:2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile
CAS No.:1356493-42-9
Molecular Formula:C₂₄H₃₂N₁₀
Molecular Weight:460.585
Hs Code.:

Synonyms:2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

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Chemical Property of 2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

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Technology Process of 2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

There total 10 articles about 2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1309831-11-5
5-Cyano-2-Chloro-N₄-(2,2,6,6-Tetramethylpiperidin-4-yl)-4-Pyrimidineamine

: 1356493-66-7
4-isopropyl-3-(1H-tetrazol-1-yl)benzenamine

: 1356493-42-9
2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

Guidance literature:: 5-Cyano-2-Chloro-N₄-(2,2,6,6-Tetramethylpiperidin-4-yl)-4-Pyrimidineamine; 4-isopropyl-3-(1H-tetrazol-1-yl)benzenamine; With toluene-4-sulfonic acid; In isopropyl alcohol; at 80 ℃; for 3h;

With ammonia; In methanol; isopropyl alcohol; at 20 ℃;

Reference yield:

: 643-28-7
2-isopropylaniline

: 1356493-42-9
2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid; sulfuric acid / 0 °C

2.1: acetic acid / 0.17 h / 20 °C

2.2: 1 h / 120 °C

2.3: 0 °C

3.1: ammonium chloride / iron / ethanol; water / 2 h / Reflux

4.1: toluene-4-sulfonic acid / isopropyl alcohol / 3 h / 80 °C

4.2: 20 °C

With sulfuric acid; nitric acid; ammonium chloride; toluene-4-sulfonic acid; acetic acid; iron; In ethanol; water; isopropyl alcohol;

Reference yield:

: 132475-93-5
2-isopropyl-5-nitroaniline

: 1356493-42-9
2-(4-isopropyl-3-(1H-tetrazol-1-yl)phenylamino)-4-(2,2,6,6-tetramethylpiperidin-4-ylamino)pyrimidine-5-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 0.17 h / 20 °C

1.2: 1 h / 120 °C

1.3: 0 °C

2.1: ammonium chloride / iron / ethanol; water / 2 h / Reflux

3.1: toluene-4-sulfonic acid / isopropyl alcohol / 3 h / 80 °C

3.2: 20 °C

With ammonium chloride; toluene-4-sulfonic acid; acetic acid; iron; In ethanol; water; isopropyl alcohol;