N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

Base Information

Chemical Name:N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine
CAS No.:1393591-54-2
Molecular Formula:C₁₇H₁₈N₄S
Molecular Weight:310.423
Hs Code.:

N<sub>2</sub>-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

Synonyms:N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

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Chemical Property of N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

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Technology Process of N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

There total 2 articles about N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 624737-93-5
5-amino-2-(benzylamino)-1,3-thiazole-4-carbonitrile

: 1393591-54-2
N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

Guidance literature:: With aluminum (III) chloride; In 1,2-dichloro-ethane; for 6h; Inert atmosphere; Reflux;
DOI:10.3998/ark.5550190.0013.329

Reference yield:

: 622-78-6
Benzyl isothiocyanate

: 1393591-54-2
N₂-benzyl-6,7-dihydro-5H-cyclopenta[b][1,3]thiazolo[4,5-e]pyridine-2,8-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 72 h / 20 - 40 °C / Inert atmosphere

2: aluminum (III) chloride / 1,2-dichloro-ethane / 6 h / Inert atmosphere; Reflux

With aluminum (III) chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,2-dichloro-ethane; 2: |Friedlaender Quinoline Synthesis;
DOI:10.3998/ark.5550190.0013.329