methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

Base Information

Chemical Name:methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate
CAS No.:225794-01-4
Molecular Formula:C₁₉H₂₃NO₉S
Molecular Weight:441.459
Hs Code.:

Synonyms:methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

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Technology Process of methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

There total 6 articles about methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 225794-00-3
methyl 2-S-(2-nitrophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

: 225794-01-4
methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

Guidance literature:: With hydrogen; platinum on activated charcoal; In methanol; Ambient temperature;
DOI:10.1002/jhet.5570360220

Reference yield: 56.0%

: 137-07-5
2-amino-benzenethiol

: 225937-33-7
methyl (3,4,5-tri-O-acetyl-β-D-arabino-hex-2-ulopyranosyl)onate bromide

: 225794-01-4
methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

Guidance literature:: With potassium carbonate; In acetone; for 2h; Heating;
DOI:10.1002/jhet.5570360220

Reference yield:

: 72933-34-7
methyl β-D-arabino-hex-2-ulopyranosonate

: 225794-01-4
methyl 2-S-(2-aminophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / conc. H₂SO₄ / 0.33 h / 60 °C

2: 98 percent / HBr, glacial AcOH / 2 h / 20 °C

3: 92 percent / K₂CO₃ / acetone / 2 h / Heating

4: 95 percent / H₂ / 5 percent Pt/C / methanol / Ambient temperature

With sulfuric acid; hydrogen bromide; hydrogen; potassium carbonate; acetic acid; platinum on activated charcoal; In methanol; acetone;
DOI:10.1002/jhet.5570360220