Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

Base Information

Chemical Name:Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate
CAS No.:509088-23-7
Molecular Formula:C₂₈H₃₃ClF₃NO₆S
Molecular Weight:604.087
Hs Code.:

Synonyms:Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

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Chemical Property of Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

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Technology Process of Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

There total 2 articles about Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 509088-94-2
2-Chloro-1-(3-iodopropyl)-4-(3-trifluoromethylphenylthio) benzene

: 102831-44-7
diethyl tert-butoxycarbonylaminomalonate

: 509088-23-7
Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

Guidance literature:: With sodium t-butanolate; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 - 80 ℃; for 5.33333h; Heating / reflux;

Reference yield:

: 509088-94-2
2-Chloro-1-(3-iodopropyl)-4-(3-trifluoromethylphenylthio) benzene

: 509088-23-7
Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

Guidance literature:: diethyl tert-butoxycarbonylaminomalonate; With sodium t-butanolate; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 80 ℃; for 0.333333h;

2-Chloro-1-(3-iodopropyl)-4-(3-trifluoromethylphenylthio) benzene; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 20 ℃; for 5h; Heating / reflux;

Reference yield:

: 509088-23-7
Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate

: 509088-38-4
2-t-butoxycarbonylamino-2-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]propyl-1,3-propanediol

Guidance literature:: Ethyl 2-t-butoxycarbonylamino-5-[2-chloro-4-(3-trifluoromethylphenylthio)]phenyl-2-ethoxycarbonylpentanoate; With lithium borohydride; In tetrahydrofuran; at 0 ℃;

With ethanol; In tetrahydrofuran; at 0 - 20 ℃;