2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

Base Information

Chemical Name:2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride
CAS No.:130450-92-9
Molecular Formula:C₅₃H₅₅ClO₉
Molecular Weight:871.467
Hs Code.:

Synonyms:2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

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Chemical Property of 2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

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Technology Process of 2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

There total 15 articles about 2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-D-xylopyranose

: 130450-92-9
2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/0008-6215(90)84242-M

Reference yield:

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 130450-92-9
2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / AgClO₄, 2,4,6-trimethylpyridine / diethyl ether / Ambient temperature

2: 1.)tris(triphenylphosphine)rhodium(I) chloride, 1,4-diazabicyclo<2.2.2>octane, 2.)HgO, HgCl₂ / 1.)EtOH-PhMe-H₂O, reflux, 8 h, 2.)acetone-water, r.t.

3: 92 percent / oxalyl chloride / CH₂Cl₂; dimethylformamide / Ambient temperature

With 1,4-diaza-bicyclo[2.2.2]octane; 2,4,6-trimethyl-pyridine; Wilkinson's catalyst; oxalyl dichloride; silver perchlorate; mercury dichloride; mercury(II) oxide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84242-M

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 130450-92-9
2,3-Di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-xylopyranosyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / oxalyl chloride / CH₂Cl₂; dimethylformamide / Ambient temperature

2: 75 percent / AgClO₄, 2,4,6-trimethylpyridine / diethyl ether / Ambient temperature

3: 1.)tris(triphenylphosphine)rhodium(I) chloride, 1,4-diazabicyclo<2.2.2>octane, 2.)HgO, HgCl₂ / 1.)EtOH-PhMe-H₂O, reflux, 8 h, 2.)acetone-water, r.t.

4: 92 percent / oxalyl chloride / CH₂Cl₂; dimethylformamide / Ambient temperature

With 1,4-diaza-bicyclo[2.2.2]octane; 2,4,6-trimethyl-pyridine; Wilkinson's catalyst; oxalyl dichloride; silver perchlorate; mercury dichloride; mercury(II) oxide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84242-M