N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

Base Information

Chemical Name:N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide
CAS No.:1192928-03-2
Molecular Formula:C₂₃H₁₉N₃O₆
Molecular Weight:433.42
Hs Code.:

Synonyms:N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

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Technology Process of N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

There total 6 articles about N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1192927-96-0
N-(3-benzamidophenylcarbamothioyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

: 1192928-03-2
N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

Guidance literature:: With copper(l) chloride; sodium hydroxide; In acetonitrile; at 120 ℃; for 0.1h; under 2585.81 Torr; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jm2013369

Reference yield:

: 4771-08-8
N-(3-nitrophenyl)benzamide

: 1192928-03-2
N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; ammonium formate / isopropyl alcohol / Inert atmosphere; Microwave irradiation

2: acetone / 1 h / Inert atmosphere; Reflux

3: copper(l) chloride; sodium hydroxide / acetonitrile / 0.1 h / 120 °C / 2585.81 Torr / Inert atmosphere; Microwave irradiation

With palladium 10% on activated carbon; ammonium formate; copper(l) chloride; sodium hydroxide; In isopropyl alcohol; acetone; acetonitrile;
DOI:10.1021/jm2013369

Reference yield:

: 76015-47-9
7-methoxy-benzo[1,3]dioxole-5-carbonyl chloride

: 1192928-03-2
N-(3-benzamidophenylcarbamoyl)-7-methoxybenzo[d][1,3]dioxole-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 0.33 h / Inert atmosphere; Reflux

2: acetone / 1 h / Inert atmosphere; Reflux

3: copper(l) chloride; sodium hydroxide / acetonitrile / 0.1 h / 120 °C / 2585.81 Torr / Inert atmosphere; Microwave irradiation

With copper(l) chloride; sodium hydroxide; In acetone; acetonitrile;
DOI:10.1021/jm2013369