[1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

Base Information

• Chemical Name: [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester
• CAS No.: 906565-33-1
• Molecular Formula: C₃₅H₂₈N₂O₄
• Molecular Weight: 540.618

Synonyms:[1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

Chemical Property of [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

Chemical Property:

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Technology Process of [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

There total 5 articles about [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

[1-benzyl-2-(1-benzyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester (906565-32-0) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester (906565-33-1)

Guidance literature:

With trichlorophosphate;

DOI:10.1016/j.tetlet.2006.04.157

Reference yield:

[2-(1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester (906565-31-9) → [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester (906565-33-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / K₂CO₃ / acetonitrile / Heating

2: 59 percent / POCl₃

With potassium carbonate; trichlorophosphate; In acetonitrile;

DOI:10.1016/j.tetlet.2006.04.157

Reference yield:

1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid (906565-30-8) → [1-benzyl-2-(1-benzyl-3-formyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester (906565-33-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: KOH / H₂O / Heating

1.2: 41 percent / H₂SO₄

2.1: 100 percent / K₂CO₃ / acetonitrile / Heating

3.1: 59 percent / POCl₃

With potassium hydroxide; potassium carbonate; trichlorophosphate; In water; acetonitrile;

DOI:10.1016/j.tetlet.2006.04.157

upstream raw materials:

[1-benzyl-2-(1-benzyl-1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

N,N-dimethyl-formamide

[2-(1H-indole-2-carbonyl)-1H-indol-3-yl]-acetic acid methyl ester

1-benzenesulfonyl-2-(3-methoxycarbonylmethyl-1H-indole-2-carbonyl)-1H-indole-3-carboxylic acid

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