Technology Process of C44H43NO
There total 5 articles about C44H43NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C43H50NO3P;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
furfural;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1016/j.dyepig.2012.03.027
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: iodine / 2.58 h / 0 - 20 °C
2.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
potassium tert-butylate; iodine;
In
tetrahydrofuran;
2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1016/j.dyepig.2012.03.027
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 32 h / 80 °C / Inert atmosphere
2.1: sodium tetrahydroborate
3.1: iodine / 2.58 h / 0 - 20 °C
4.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
With
sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate; iodine; sodium carbonate;
In
tetrahydrofuran; water;
1.1: Suzuki coupling / 4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1016/j.dyepig.2012.03.027