dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate

Base Information

• Chemical Name: dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate
• CAS No.: 1352724-41-4
• Molecular Formula: C₂₆H₃₀FO₁₁P
• Molecular Weight: 568.49

Synonyms:dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate

Chemical Property of dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate

Chemical Property:

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Technology Process of dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate

There total 2 articles about dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

phosphoric acid dibenzyl ester (1623-08-1) + 3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranosyl bromide (34245-85-7) → dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate (1352724-41-4)

Guidance literature:

With silver carbonate; In acetonitrile; Inert atmosphere; Darkness;

DOI:10.1002/anie.201103924

Reference yield:

dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranosyl)phosphate (209005-14-1) → dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate (1352724-41-4)

Guidance literature:

With phosphoric acid dibenzyl ester; In toluene; Inert atmosphere;

DOI:10.1039/c4ob00235k

Reference yield: 65.0%

dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate (1352724-41-4) → dibenzyl (2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate (1352724-45-8)

Guidance literature:

With methanol; sodium; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201103924

upstream raw materials:

phosphoric acid dibenzyl ester

3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranosyl bromide

dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranosyl)phosphate

Downstream raw materials:

dibenzyl (2-deoxy-2-fluoro-β-D-glucopyranosyl) phosphate

dibenzyl (3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-glucopyranosyl)phosphate

benzyl benzyl-(2-deoxy-2-fluoro-α-D-glucopyranosyl)phosphate

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