3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid

Base Information

• Chemical Name: 3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid
• CAS No.: 124841-26-5
• Molecular Formula: C₂HF₃O₂*C₁₄H₁₆N₄O₃S
• Molecular Weight: 434.396

Synonyms:3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid

Chemical Property of 3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid

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Technology Process of 3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid

There total 1 articles about 3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

N-(2-hydroxyphenyl)-3-oxobutanamide (22016-02-0) + trifluoroacetic acid (76-05-1) + 3-methylthio-1,2,4-triazine (28735-21-9) → 3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid (124841-26-5)

Guidance literature:

In chloroform; 1) reflux, 2) rt, 50 hr;

DOI:10.1016/S0040-4039(00)80316-0

Reference yield: 75.0%

3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid (124841-26-5) → 3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-7-nitroso-3a,4,7,7a-tetrahydro-1H,3H-1,4,6,7-tetraaza-inden-2-one (124841-28-7)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 5 ℃; for 0.25h;

DOI:10.1016/S0040-4039(00)80316-0

Reference yield:

3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one; compound with trifluoro-acetic acid (124841-26-5) → 3-Acetyl-1-(4-hydroxy-phenyl)-5-methylsulfanyl-7-nitroso-1,3,3a,4,7,7a-hexahydro-1,4,6,7-tetraaza-inden-2-one

Guidance literature:

With hydrogenchloride; sodium nitrite; at 5 ℃; for 0.25h; Yield given;

DOI:10.1007/BF00978446

upstream raw materials:

N-(2-hydroxyphenyl)-3-oxobutanamide

trifluoroacetic acid

3-methylthio-1,2,4-triazine

Downstream raw materials:

3-Acetyl-1-(2-hydroxy-phenyl)-5-methylsulfanyl-7-nitroso-3a,4,7,7a-tetrahydro-1H,3H-1,4,6,7-tetraaza-inden-2-one

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