(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

Base Information

Chemical Name:(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol
CAS No.:1115267-08-7
Molecular Formula:C₄₃H₅₂O₇Si
Molecular Weight:708.967
Hs Code.:

(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

Synonyms:(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

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Chemical Property of (1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

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Technology Process of (1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

There total 1 articles about (1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1115266-92-6
(2R,3R,5R,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanone

: 1115267-08-7
(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2008.11.055

Reference yield: 92.0%

: 1115267-08-7
(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

: 1115267-17-8
C₄₃H₅₄O₇Si

Guidance literature:: (1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2008.11.055

Reference yield: 86.0%

: 1115267-08-7
(1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol

: 1115267-09-8
(1R,2S,4R,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-1-methyl-5-cyclohexen-1,2-diol

Guidance literature:: (1S,2S,3R,5S,Z)-5-{3-[2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl]-1-[(2-methoxyethoxy)methoxy]-2-propen-2-yl}-2,3-epoxy-2-methylcyclohexanol; With aluminum isopropoxide; In toluene; for 1.5h; Reflux;

With hydrogenchloride; In water; toluene; at 20 ℃;
DOI:10.1016/j.tet.2008.11.055