C₂₃H₂₇NO₄

Base Information

Chemical Name:C₂₃H₂₇NO₄
CAS No.:1259067-12-3
Molecular Formula:C₂₃H₂₇NO₄
Molecular Weight:381.472
Hs Code.:

C<sub>23</sub>H<sub>27</sub>NO<sub>4</sub>

Synonyms:C₂₃H₂₇NO₄

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Chemical Property of C₂₃H₂₇NO₄

Chemical Property:

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Technology Process of C₂₃H₂₇NO₄

There total 14 articles about C₂₃H₂₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1259067-08-7
C₂₇H₃₃Cl₃N₂O₅

: 1259067-12-3
C₂₃H₂₇NO₄

Guidance literature:: With lithium hydroxide; In water; tert-butyl alcohol; at 50 - 100 ℃; for 108h; Inert atmosphere;
DOI:10.1021/ol1026602

Reference yield: 61.0%

: C₂₇H₃₃Cl₃N₂O₅

: 1259067-12-3
C₂₃H₂₇NO₄

Guidance literature:: With lithium hydroxide; In tert-butyl alcohol; at 50 - 100 ℃; for 108h; Inert atmosphere;
DOI:10.1002/ejoc.201200523

Reference yield:

: 160836-05-5
C₂₁H₂₆O₅

: 1259067-12-3
C₂₃H₂₇NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: o-xylene / 123 h / 20 - 160 °C / Inert atmosphere; Molecular sieve; Sealed tube

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / o-xylene / 1.5 h / 140 °C / Inert atmosphere

4: lithium hydroxide / water; tert-butyl alcohol / 108 h / 50 - 100 °C / Inert atmosphere

With potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In dichloromethane; o-xylene; water; tert-butyl alcohol; 1: Claisen rearrangement / 3: Overman rearrangement;
DOI:10.1021/ol1026602