C₂₉H₂₅N₃O₈S

Base Information

• Chemical Name: C₂₉H₂₅N₃O₈S
• CAS No.: 218960-28-2
• Molecular Formula: C₂₉H₂₅N₃O₈S
• Molecular Weight: 575.599
• Mol file: 218960-28-2.mol

Synonyms:C₂₉H₂₅N₃O₈S

Chemical Property of C₂₉H₂₅N₃O₈S

Chemical Property:

Purity/Quality:

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Technology Process of C₂₉H₂₅N₃O₈S

There total 1 articles about C₂₉H₂₅N₃O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-di-O-acetyl-3,5-di-O-benzoyl-β-D-ribofuranoside (71080-18-7) + 5-(3'-thienyl)cytosine → C29H25N3O8S (218960-28-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; Yield given; Multistep reaction; 1.) DMF, RT, 1 h, 2.) DMF, 70 deg C, 2 h;

Reference yield: 75.0%

C29H25N3O8S (218960-28-2) → C27H23N3O7S (218960-30-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 36h; Ambient temperature;

Reference yield:

C29H25N3O8S (218960-28-2) → C27H22ClN3O6S (218960-32-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / aq. HCl / dioxane / 36 h / Ambient temperature

2: 64 percent / SOCl₂ / acetonitrile / 8 h / 70 °C

With hydrogenchloride; thionyl chloride; In 1,4-dioxane; acetonitrile;

upstream raw materials:

1,2-di-O-acetyl-3,5-di-O-benzoyl-β-D-ribofuranoside

Downstream raw materials:

C₂₇H₂₃N₃O₇S

C₂₇H₂₂ClN₃O₆S