bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

Base Information

Chemical Name:bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate
CAS No.:132541-45-8
Molecular Formula:C₂₀H₃₅O₆P
Molecular Weight:402.468
Hs Code.:

Synonyms:bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

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Chemical Property of bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

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Technology Process of bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

There total 1 articles about bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 81172-89-6
terephthalaldehyde mono(diethylacetal)

: 13086-84-5
di-tert-butyl phosphite

: 132541-45-8
bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

Guidance literature:: With aluminum oxide; Ambient temperature;
DOI:10.1021/jm00109a008

Reference yield: 100.0%

: 132541-45-8
bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

: 132541-46-9
bis(1,1-dimethylethyl) <(4-formylphenyl)hydroxymethyl>phosphonate

Guidance literature:: With hydrogenchloride; In chloroform; for 0.333333h; Ambient temperature;
DOI:10.1021/jm00109a008

Reference yield:

: 132541-45-8
bis(1,1-dimethylethyl) <<4-(diethoxymethyl)phenyl>hydroxymethyl>phosphonate

: 146745-45-1
methyl 4-<(di-tert-butylphosphono)hydroxymethyl>-D,L-phenylalaninate

Guidance literature:: Multi-step reaction with 3 steps

1: 1 N HCl / CHCl₃ / Ambient temperature

2: 57 percent / NaOMe / 1) -78 deg C, 5 min, 2) 0 deg C, 1 h

3: 92 percent / H₂ / 10percent Pd/C / methanol / 3 h / 2068.6 Torr

With hydrogenchloride; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jo00058a009