1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

Base Information

Chemical Name:1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane
CAS No.:916330-73-9
Molecular Formula:C₅₈H₅₈O₁₆
Molecular Weight:1011.09
Hs Code.:

Synonyms:1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

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Chemical Property of 1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

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Technology Process of 1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

There total 7 articles about 1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 916330-61-5
5-(benzyloxy)-2-(4-hydroxyphenyl)-7-(methoxymethoxy)-4H-chromen-4-one

: 109789-39-1
pentaethylene glycol dimesylate

: 916330-73-9
1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Heating;
DOI:10.1021/jm060593+

Reference yield: 43.0%

: 916330-73-9
1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

Guidance literature:

Reference yield:

: 916330-66-0
5-hydroxy-7-methoxymethoxy-2-(4-allyloxyphenyl)-4H-chromen-4-one

: 916330-73-9
1,16-bis[4-((5-benzyloxy-7-methoxymethoxy)-4H-chromen-4-on-2-yl)phenyl]-1,4,7,10,13,16-hexaoxahexadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / K₂CO₃ / dimethylformamide / 2 h / Heating

2: 78 percent / Pd(PPh₃)4; K₂CO₃ / methanol / 2 h / Heating

3: 43 percent / K₂CO₃ / dimethylformamide / Heating

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060593+