Technology Process of C15H12ClN5O
There total 7 articles about C15H12ClN5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: dmap; triethylamine / dichloromethane / 48 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / ethanol / 48 h / 50 °C / 2585.81 Torr
3: hydrogenchloride / 1,4-dioxane / 5 h / 20 °C
4: dihydrogen peroxide; sodium hydroxide / water / 96 h / 75 °C / pH 7-8
5: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
6: hydrazine hydrate / ethanol / 0.33 h / 85 °C
7: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
With
hydrogenchloride; dmap; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; dihydrogen peroxide; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dihydrogen peroxide; sodium hydroxide / water / 96 h / 75 °C / pH 7-8
2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
3: hydrazine hydrate / ethanol / 0.33 h / 85 °C
4: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; dihydrogen peroxide; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;