{2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

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Chemical Name:{2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane
CAS No.:500102-36-3
Molecular Formula:C₂₆H₄₂O₄Si
Molecular Weight:446.703
Hs Code.:

Synonyms:{2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

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Chemical Property of {2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

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Technology Process of {2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

There total 3 articles about {2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 500102-35-2
(2S,3S)-2-((E)-Buta-1,3-dienyl)-5-triisopropylsilanyloxy-pentane-1,3-diol

: 500102-36-3
{2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

Guidance literature:: With camphor-10-sulfonic acid; In 1,2-dichloro-ethane; Heating;
DOI:10.1016/S0040-4039(02)01662-3

Reference yield:

: 111998-84-6
3-(triisopropylsiloxy)propanal

: 500102-36-3
{2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Bu₂BOTf; Et₃N / -78 °C

1.2: LiBH₄ / pH 7

1.3: H₂O₂ / H₂O

2.1: 80 percent / CSA / 1,2-dichloro-ethane / Heating

With di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; triethylamine; In 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(02)01662-3

Reference yield:

: 220944-25-2
(4R,5S)-4-methyl-5-phenyl-3-((2E,4E)-1-oxo-2,4-hexadienyl)-2-oxazolidinone

: 500102-36-3
{2-[(4S,5S)-5-((E)-Buta-1,3-dienyl)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-ethoxy}-triisopropyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Bu₂BOTf; Et₃N / -78 °C

1.2: LiBH₄ / pH 7

1.3: H₂O₂ / H₂O

2.1: 80 percent / CSA / 1,2-dichloro-ethane / Heating

With di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; triethylamine; In 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(02)01662-3