Technology Process of C19H22OSi
There total 5 articles about C19H22OSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C21H26O3Si;
With
water; ammonium formate;
In
N,N-dimethyl-formamide;
at 23 ℃;
for 0.666667h;
Inert atmosphere;
palladium bis[bis(diphenylphosphino)ferrocene] dichloride;
In
N,N-dimethyl-formamide;
at 23 ℃;
for 16h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.08 h / Cooling with acetone-dry ice; Inert atmosphere
1.2: 1.83 h / Inert atmosphere
1.3: Inert atmosphere
2.1: methanol; dichloromethane / 12.5 h / 5 °C / Cooling with ice-water; Inert atmosphere
2.2: 0.42 h / Inert atmosphere
2.3: 0.92 h / Inert atmosphere
3.1: triethylamine / Inert atmosphere
3.2: Lipase Amano "PS" IM / 20 h / 23 °C / Inert atmosphere
4.1: water; ammonium formate / N,N-dimethyl-formamide / 0.67 h / 23 °C / Inert atmosphere
4.2: 16 h / 23 °C / Inert atmosphere
With
n-butyllithium; water; ammonium formate; triethylamine;
In
tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / Inert atmosphere
1.2: Lipase Amano "PS" IM / 20 h / 23 °C / Inert atmosphere
2.1: water; ammonium formate / N,N-dimethyl-formamide / 0.67 h / 23 °C / Inert atmosphere
2.2: 16 h / 23 °C / Inert atmosphere
With
water; ammonium formate; triethylamine;
In
N,N-dimethyl-formamide;
