Technology Process of C48H86N6O10S2Si2
There total 11 articles about C48H86N6O10S2Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; lithium hydroxide;
In
tetrahydrofuran; tert-butyl alcohol;
at 0 ℃;
for 1h;
DOI:10.1039/c0cc01200a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-ethyl-N,N-diisopropylamine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
2: tetrahydrofuran / 0 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V) / dichloromethane / 0 - 20 °C / Inert atmosphere
4: tetrahydrofuran / 0 °C / Inert atmosphere
5: lithium hydroxide / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 0 °C
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V); lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/chem.201203667
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; sodium nitrite / water / 0.5 h / 0 - 40 °C
2: tetrahydrofuran / 0 °C / Inert atmosphere
3: lithium hydroxide / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 0 °C
With
acetic acid; lithium hydroxide; sodium nitrite;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1002/chem.201203667
