C₂₆H₂₆BrN

Base Information

• Chemical Name: C₂₆H₂₆BrN
• CAS No.: 1446741-29-2
• Molecular Formula: C₂₆H₂₆BrN
• Molecular Weight: 432.403
• Mol file: 1446741-29-2.mol

Synonyms:C₂₆H₂₆BrN

Chemical Property of C₂₆H₂₆BrN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₆BrN

There total 7 articles about C₂₆H₂₆BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1,4-bromoiodobenzene (589-87-7) + C26H34BNO2 (1385798-22-0) → C26H26BrN (1446741-29-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; toluene; Reflux;

Reference yield:

C20H23N (1385798-18-4) → C26H26BrN (1446741-29-2)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2: palladium dichloride; sodium acetate / toluene / 8 h / Reflux

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; 1,4-dioxane / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; potassium carbonate; palladium dichloride; In 1,4-dioxane; N,N-dimethyl-formamide; toluene;

Reference yield:

C20H22BrN (1385798-20-8) → C26H26BrN (1446741-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium dichloride; sodium acetate / toluene / 8 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; 1,4-dioxane / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; potassium carbonate; palladium dichloride; In 1,4-dioxane; toluene;

upstream raw materials:

C₂₀H₂₃N

C₂₀H₂₂BrN

1,4-bromoiodobenzene

C₂₆H₃₄BNO₂

Downstream raw materials:

C₃₂H₃₈BNO₂

Refernces