2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

Base Information

Chemical Name:2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol
CAS No.:413578-26-4
Molecular Formula:C₃₁H₃₀N₂O₆
Molecular Weight:526.589
Hs Code.:

Synonyms:2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

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Chemical Property of 2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

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Technology Process of 2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

There total 19 articles about 2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 897918-47-7
[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethyl triphenylmethyl ether

: 413578-26-4
2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

Guidance literature:: With hydrogenchloride; methanol; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/jo060501o

Reference yield: 87.0%

: 413578-25-3
2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethyl acetate

: 413578-26-4
2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

Guidance literature:: With methanol; potassium carbonate; at 20 ℃;

Reference yield:

: 413578-20-8
ethyl (4-hydroxy-2-nitronaphthalen-1-yl)acetate

: 413578-26-4
2-[4-benzyloxy-2-(5,6,7-trimethoxyindole-2-carboxamido)naphthalen-1-yl]ethanol

Guidance literature:: Multi-step reaction with 6 steps

1: K₂CO₃ / acetone / 20 °C

2: DIBAL-H / tetrahydrofuran / 0.25 h / 0 °C

3: 0.21 g / pyridine / 20 °C

4: H₂ / PtO₂ / tetrahydrofuran / 1 h / 20 °C / 2844.31 Torr

5: 37 percent / 1-hydroxybenzotriazole; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide HCl; pyridine / 120 h / 20 - 60 °C

6: K₂CO₃ / methanol / 20 °C

With pyridine; hydrogen; diisobutylaluminium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; platinum(IV) oxide; In tetrahydrofuran; methanol; acetone;
DOI:10.1021/jm050179u