2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

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Chemical Name:2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione
CAS No.:1259858-95-1
Molecular Formula:C₅₈H₆₈N₂O₂S₄
Molecular Weight:953.454
Hs Code.:

Synonyms:2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

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Chemical Property of 2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

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Technology Process of 2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

There total 3 articles about 2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2-(5'-hexyl-[2,2']bithiophenyl-5-yl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 266357-54-4
3,6?bis(4?bromophenyl)?2,5?dihexylpyrrolo[3,4?c]pyrrole?1,4(2H,5H)?dione

: 1259858-95-1
2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; at 80 ℃; Inert atmosphere;
DOI:10.1021/cm202852f

Reference yield:

: 111-25-1
1-bromo-hexane

: 1259858-95-1
2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 40 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 80 °C / Inert atmosphere

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 2: Suzuki coupling;
DOI:10.1021/cm202852f

Reference yield:

: 84632-54-2
3,6-bis(4-bromophenyl)-2,5-dihydropyrrolo[3, 4-c]pyrrole-1,4-dione

: 1259858-95-1
2,5-dihexyl-3,6-bis[4-(5-hexyl-2,2'-bithiophene-5-yl)phenyl]pyrrolo[3,4-c]-pyrrole-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 40 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 80 °C / Inert atmosphere

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 2: Suzuki coupling;
DOI:10.1021/cm202852f